Lubricating Agents in Pharmaceutical Formulation

What is a Lubricant?

An excipient used in tablet & capsule formulation to reduce friction between powder/granules and the die wall during compression & ejection.

Lubricating Agents in Pharmaceutical Formulation

Standard Usage Range & Maximum Limit

Lubricant ,Standard Range (% w/w) , Maximum Limit (% w/w)

Magnesium stearate - 0.25 -1.0 (Max.-1.0%)

Calcium stearate 0.5 – 1.5 (Max.1.5%)

Stearic acid 0.5 – 2.0 (Max. 2.0%)

Talc 1.0 – 5.0. ( Max. 5.0%)

General rule: In most formulations, total lubricant ≤1%, except talc (up to 5%)

Golden Rules of Lubricant Use

🟢 Add Last → Only at the final blending stage.

🟢 Mix Less → Mix gently for 2–5 minutes to prevent over-coating.

Why Not Added During Wet Mixing?

💧 Hydrophobic → Repels binder solution, affects granule formation.

💧 Loses lubricating property → gets washed out during granulation.

💧 Produces weak granules → causes capping, lamination, poor hardness.

Why Not Exceed Maximum Limit?

🔻 Hydrophobic Film Formation → Blocks water penetration → poor disintegration & dissolution.

🔻 Reduced Hardness → Over-lubrication weakens inter-particle bonding.

🔻 Bioavailability Issues → Slower dissolution → therapeutic failure.

🔻 Regulatory Failure → Tablets may not meet pharmacopeial QTPP (Quality Target Product Profile).

Practical Example

👉 In Paracetamol tablets:

Magnesium stearate (0.25–0.5% w/w) is added last, mixed for 2–3 min only.

If used >1% or mixed too long → tablet shows softness, delayed disintegration & dissolution.

Quick Summary

✔️ Lubricant range: 0.25–5% (depending on type).

✔️ Maximum limit: usually ≤1%, except talc (≤5%).

✔️ Golden rule: Add last, Mix less.

✔️ Never in wet mixing: hydrophobic → weak granules.

✔️ Exceeding max limit → poor hardness, disintegration & dissolution.

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